第1章 緒論 1 Chapter 1 Introduction 1 1.1 無(wú)機(jī)化學(xué)實(shí)驗(yàn)的目的 1 1.1 Objectives of Inorganic Chemistry Experiment 1 1.2 無(wú)機(jī)化學(xué)實(shí)驗(yàn)的學(xué)習(xí)方法 2 1.2 Methods to Study Inorganic Chemistry Experiment 4 1.3 學(xué)生實(shí)驗(yàn)守則 6 1.3 Laboratory Rules for Students 6 1.4 實(shí)驗(yàn)室安全守則 8 1.4 Laboratory Safety Rules 9 1.5 化學(xué)實(shí)驗(yàn)常用儀器介紹 12 1.5 Frequently Used Laboratory Equipment 16
第2章 基本操作訓(xùn)練 20 Chapter 2 Basic Laboratory Techniques 20 無(wú)機(jī)化學(xué)實(shí)驗(yàn)基本操作 20 Basic Laboratory Techniques for Inorganic Chemistry Experiment 20 2.1 常用玻璃儀器的洗滌和干燥 20 2.1 Cleaning and Drying Glassware 22 2.2 加熱方法 25 2.2 Heating 28 2.3 容量?jī)x器及其使用 31 2.3 Volumetric Glassware 34 2.4 化學(xué)試劑及其取用 39 2.4 Transferring Chemical Reagents 39 2.5 溶液的配制 41 2.5 Preparing Solutions 41 2.6 氣體的發(fā)生、凈化、干燥和收集 42 2.6 Preparing, Purifying, Drying and Collecting Gases 44 2.7 蒸發(fā)（濃縮）、結(jié)晶（重結(jié)晶） 47 2.7 Evaporation (Concentration) and Crystallization (Recrystallization) 47 2.8 結(jié)晶（沉淀）的分離和洗滌 49 2.8 Separating a Liquid or Solution From a Solid 52 2.9 試紙的使用 56 2.9 Using Test Paper 56 2.10 誤差與數(shù)據(jù)處理 58 2.10 Errors and Treatment of Data 62 2.11 有效數(shù)字 68 2.11 Significant Figures 70 實(shí)驗(yàn)部分 74 Experiments 74 實(shí)驗(yàn)1 滴定操作練習(xí) 74 Experiment 1 Titrimetric Analysis 76 實(shí)驗(yàn)2 酸堿滴定 79 Experiment 2 Acid-Base Titration 80 實(shí)驗(yàn)3 EDTA標(biāo)準(zhǔn)溶液的配制與標(biāo)定 83 Experiment 3 Preparation and Standardization of an EDTA Solution 84 實(shí)驗(yàn)4 水中鈣、鎂含量的測(cè)定（配位滴定法） 86 Experiment 4 An Analysis of Concentrations of Calcium and Magnesium Ions in a Water Sample 87
第3章 常數(shù)測(cè)定 89 Chapter 3 Determination of the Constant 89 實(shí)驗(yàn)5 化學(xué)反應(yīng)速率和活化能 89 Experiment 5 Determination of a Rate Law and Activation Energy 92 實(shí)驗(yàn)6 弱酸電離常數(shù)測(cè)定（pH法） 95 Experiment 6 Determination of Ionization Constant of Acetic Acid 96 實(shí)驗(yàn)7 硫酸鋇溶度積的測(cè)定（電導(dǎo)法） 98 Experiment 7 Determination of the Solubility Product Constant of Barium Sulfate 100 實(shí)驗(yàn)8 磺基水楊酸鐵配合物的組成及穩(wěn)定常數(shù)的測(cè)定 104 Experiment 8 Determination of the Composition and the Stability Constant of an Iron(Ⅲ)-Sulfosalicylate Complex 106 實(shí)驗(yàn)9 氧化還原反應(yīng) 110 Experiment 9 Oxidation-Reduction Reactions 111
第4章 化合物的制備與提純 114 Chapter 4 Preparation and Purification of Compounds 114 實(shí)驗(yàn)10 硫酸銅的提純 114 Experiment 10 Purification of Copper (Ⅱ) Sulfate 116 實(shí)驗(yàn)11 氯化鈉的提純 118 Experiment 11 Purification of Sodium Chloride 119 實(shí)驗(yàn)12 氯化鉀的提純 122 Experiment 12 Purification of Potassium Chloride 123 實(shí)驗(yàn)13 硝酸鉀的制備與提純 126 Experiment 13 Preparation and Purification of Potassium Nitrate 127 實(shí)驗(yàn)14 明礬的制備 130 Experiment 14 Synthesis of Potassium Alum 131 實(shí)驗(yàn)15 莫爾鹽（硫酸亞鐵銨）的制備 134 Experiment 15 Synthesis of Mohr’s Salt (Ammonium Ferrous Sulfate) 135 實(shí)驗(yàn)16 草酸配合物的合成 138 Experiment 16 Synthesis of Oxalate Complexes 139 實(shí)驗(yàn)17 硫代硫酸鈉的制備 141 Experiment 17 Preparation of Sodium Thiosulfate 143
第5章 元素及其化合物的性質(zhì) 145 Chapter 5 Properties of Elements and Compounds 145 實(shí)驗(yàn)18 s區(qū)元素及其化合物 145 Experiment 18 Elements in s-block and Their Compounds 147 實(shí)驗(yàn)19 鹵素及其化合物 151 Experiment 19 Halogens and Their Compounds 155 實(shí)驗(yàn)20 過(guò)氧化氫和硫的化合物 159 Experiment 20 Hydrogen Peroxide and Compounds of Sulfur 163 實(shí)驗(yàn)21 氮和磷 167 Experiment 21 Nitrogen and Phosphorus 171 實(shí)驗(yàn)22 ds區(qū)元素的化合物 177 Experiment 22 Elements in ds-block and Their Compounds 180 實(shí)驗(yàn)23 鈦、釩、鉻和錳的化合物 184 Experiment 23 Compounds of Ti, V, Cr and Mn 187 實(shí)驗(yàn)24 鐵、鈷、鎳的化合物 192 Experiment 24 Compounds of Fe, Co and Ni 196 實(shí)驗(yàn)25 配合物 202 Experiment 25 Coordination Compounds 203
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